Skip to main content
Get your brand new Wikispaces Classroom now
and do "back to school" in style.
Pages and Files
list of experiments
Solubility book (3rd Edn)
[add embedded ChemSpider image JCB]
To measure the solubility of 2,6-dicholobenzaldehyde in benzene and DMSO using SAMS method.
[also do density method to compare JCB]
Procedure: [should not have colon JCB]
There were 4 vials made. 2 of them were a saturated solution of 2,6-dicholobenzaldehyde in benzene and the other 2 were a saturated solution of 2,6-dicholobenzaldehyde
in DMSO. All vials were parafilmed and vortexed. Then they were placed in the temperature controlled thermostat
17:15 Turn on the temperature contol bath and set it to 46 C
17:20 Labeled four 1 dram screw cap vials 1-4.
[Are you sure these are 1 dram and not 0.5 dram? JCB]
17:25 Placed 2,6-dicholobenzaldehyde into the vials.
17:30 Pipetted out a small volume of benzene into vials 1 and 2. Vortexed the vials for about a minute and made sure some of the solid remained undissolved.
17:35 Pipetted out a small volume of DMSO into vials 3 and 4. Vortexed the vials for about a minute and made sure some of the solid remained undissolved.
17:45 Parafilmed all the vials tightly.
17:51 Placed the vials into a temprature controlled water bath at 46 C
18:09 Temperature changed in the thermostat water bath to 25 C. 2,6-dicholobenzaldehyde in all 4 vials had dissolved at 46 C
[did you observe solid coming out after sonicating for a few seconds? JCB]
help on how to format text
Turn off "Getting Started"