list of experiments

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Summary Solubility Data (CC0)
SolubilitiesSum Spreadsheet (**Read these instruction before adding data**) (Chemicalize version - hover over names to view structures)
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Alternate Solubility Web Query Interface That Accepts GET Queries (Andrew Lang)
More Web Services (Pierre Lindenbaum and Egon Willighagen)
Visualizing Chemical Space (Rajarshi Guha)
PCA Chemical Space (Andrew Lang)
CDK Descriptor Chemical Space (Andrew Lang)
Solubility Prediction (Rajarshi Guha)
List a summary of all measurements for a solute in a table via simple URL(XML version) (Andrew Lang)
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ONS solubility challenge as a data source in ChemSpider - see description (Tony Williams)
Summary of all measurements (Andrew Lang)
Outliers (Andrew Lang)
ONSgrid checklist

List of Experiments on this wiki

EXP359 Recrystallization of benzoic acid from water with a pentane wash using the sintered glass funnel method. - Matthew McBride
EXP358 Recrystallization of caffeine from toluene with a pentane wash using the sintered glass funnel method. - Matthew McBride
EXP357 Measurement of the solubility of Cinnamic acid in 10% ethanol in pentane. - Ene Anteyi
EXP355 Examination of the ability of pentane to wash 1:1 ethanol/water(vol) from trans-cinnamic acid crystals. - Matthew McBride
EXP354 Examination of layer separation of water in the ethanol/pentane binary solvent system. - Matthew McBride
EXP353 Recrystallization of trans-dibenzalacetone from ethanol using the sintered glass funnel method. - Matthew McBride
EXP352 Recrystallization of trans-cinnamic acid from cyclohexane using the sintered glass funnel method. - Matthew McBride
EXP351 Recrystallization of benzoic acid from n-hexane using the sintered glass funnel method. - Matthew McBride
EXP350 Recrystallization of trans-cinnamic acid from 1:1 ethanol/water(vol) and washing with pentane using the sintered glass funnel method. - Rani Saba
EXP349 Recrystallization of caffeine with 10% trans-cinnamic acid impurity from 1-octanol and washing with pentane at 0.75M concentration using the heat gun and a test tube with the sintered glass funnel method. - Unnati Hajari
EXP348 Recrystallization of caffeine with 50% trans-cinnamic acid impurity from 1-octanol and washing with pentane at 0.75M concentration using the heat gun and a test tube with the sintered glass funnel method. - Rani Saba
EXP347 Recrystallization of caffeine from 1-octanol and washing with pentane at 0.75M concentration using the heat gun and a test tube with the sintered glass funnel method. - Paris Dayon Favors II
EXP346 Recrystallization of caffeine from 1-octanol and washing with pentane at 1.0M concentration using the sintered glass funnel method. - Matthew McBride
EXP345 Recrystallization of salicylic acid in 1-octanol using pentane to wash the crystals. - Hieu Nguyen
EXP344 Recrystallization of trans-cinnamic acid from 1-octanol and washing with pentane at 1.5M, 0.75M and 0.25M concentrations using the centrifuge method. - Rani Saba
EXP343 Recrystallization of caffeine from 1-octanol and washing with pentane at 1.5M, 0.75M and 0.25M concentrations using the centrifuge method. - Matthew McBride
EXP342 Recrystallization of caffeine from 1-octanol and washing with pentane at 2.0M, 0.75M and 0.25M concentrations. - Matthew McBride
EXP341 Determination of the solubility of phenanthrene-9-carboxaldehyde in chloroform by the SAMS HNMR method using the shake flask method to dissolve. - Hieu Nguyen
EXP340 Determination of the solubility of trans-cinnamic acid in methanol by using the density method. - Linh Bui
EXP339 Determination of the solubility of trans-cinnamic acid in methanol by using the density method. - Hieu Nguyen
EXP338 Determination of the solubility of phenanthrene-9-carboxaldehyde in ethyl acetate and benzene by the SAMS HNMR method using the shake flask method to dissolve. - Matthew McBride
EXP337 Determination of the solubility of phenanthrene-9-carboxaldehyde in THF and methanol by the SAMS HNMR method using the shake flask method to dissolve. - Matthew McBride
EXP336 Determination of the solubility of trans-dibenzalacetone in water and 1-octanol at 25°C using UV/Vis Spectroscopy and the Shake Flask Method. - Matthew McBride
EXP335 Determination of the LogP of trans-dibenzalacetone using 10% and 1% saturated 1-octanol in pure water. - Matthew McBride
EXP334 Determination of room temperature solubility of cinnamic acid in water, octanol, hexane, and cyclohexane - Rida Atif
EXP333 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - Matthew McBride
EXP332 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - Matthew McBride
EXP331 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - Matthew McBride
EXP330 Determination of room temperature solubility of cinnamic acid in hexane and cyclohexane - Rida Atif
EXP329 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - Matthew McBride
EXP328 Determination of the solubility of trans-dibenzalacetone in water and 1-octanol at 25°C using UV/Vis Spectroscopy and the Shake Flask Method. - Matthew McBride
EXP327 Determination of room temperature solubility of benzoic acid in ethanol/water 30:70 volume - Rida Atif
EXP326 Determination of room temperature solubility of benzoic acid in ethanol/water mixtures of 30:70, 40:60, and 50:50 volumes - Rida Atif
EXP325 Determination of the recrystallization yield of trans-dibenzalacetone in n-hexane. - Matthew McBride
EXP324 Determination of the solubility of trans-dibenzalacetone in n-hexane, cyclohexane, methanol, 2-propanol and an ethanol/water mixture (50:50vol) by the SAMS HNMR method using the shake flask method to dissolve. - Matthew McBride
EXP323 Determination of room temperature solubility of benzoic acid in ethanol/water mixtures of 40:60, 50:50, 60:40 volumes as well as pure ethanol, and trans-dibenzalacetone in pure ethanol - Rida Atif and Matthew McBride
EXP322 Determination of the recrystallization yield of trans-dibenzalacetone in ethanol/water (50:50vol). - Matthew McBride
EXP321 Determination of the recrystallization yield of trans-dibenzalacetone in ethanol. - Matthew McBride
EXP320 Determination of the solubility at room temperature of benzoic acid in ethanol/water(40:60) - Rida Atif
EXP319 Determination of the recrystallization yield of benzoic acid in ethanol/water(12:20) - Rida Atif
EXP318 Determination of the recrystallization yield of benzoic acid in ethanol/water(40:60)vol - Rida Atif
EXP317 Determination of the recrystallization yield of benzoic acid in ethanol/water(12:20) - Rida Atif
EXP316 Determination of the recrystallization yield of cinnamic acid in carbon tetrachloride - Rida Atif
EXP315 Determination of the recrystallization yield of benzoic acid in carbon tetrachloride - Rida Atif
EXP314 Synthesis of trans-dibenzalacetone from acetone and benzaldehyde in an ethanol solvent and purifying by recrystallization from ethanol. - Matthew McBride
EXP313 Determination of the solubility of trans-dibenzalacetone in diethyl ether and acetone by SAMS HNMR using the shake flask method to dissolve. - Matthew McBride
EXP312 Determination of the recrystallization yield of cinnamic acid in benzene - Rida Atif
EXP311 Determination of the solubility of trans-dibenzalacetone in methanol, cyclohexanol, and acetonitrile by SAMS HNMR using the shake flask method to dissolve. - Matthew McBride
EXP310 Determination of the recrystallization yield of cinnamic acid in n-hexane - Rida Atif
EXP309 Determination of the recrystallization yield of cinnamic acid in cyclohexane - Rida Atif
EXP308 Determine the solubility of benzene, THF, Cyclohexane, Cyclohexanone and Toluene by SAMS NMR using the Shake Flate method to dissolve. - Matthew McBride
EXP307 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. - Matthew McBride
EXP306 Determination of the recrystallization yield of benzoic acid in hexane - Rida Atif
EXP305 Determination of the recrystallization yield of benzoic acid in cyclohexane - Rida Atif
EXP304 Determination of the recrystallization yield of benzoic acid in ethanol/water (40:60) - Rida Atif
EXP303 Determination of the recrystallization yield of benzoic acid in benzene - Rida Atif
EXP302 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. - Matthew McBride
EXP301 Determination of the solubility of trans-dibenzalacetone in ethyl acetate, ethanol, and hexanes by the SAMS HNMR method using the shake flask method to dissolve. - Matthew McBride
EXP300 Purification of trans-dibenzalacetone by recrystallization from ethanol. - Matthew McBride
EXP299 Determination of the recrystallization yield of benzoic acid in benzene - Rida Atif
EXP298 Determination of the recrystallization yield of benzoic acid in benzene - Rida Atif
EXP297 Determine the solubility of n-[(e)-(4-chlorophenyl)methylene]aniline in ethanol, acetonitrile, benzene, hexane, and THF by the SAMS NMR method, dissolved using shake plate method. - Mark Mangir
EXP296 Determination of the solubility of cinnamic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and [[#|polyethylene glycol]] (PEG-400, average of 9 EG units) utilizing the shake flask method - Valentine Anyiam
EXP295 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and [[#|polyethylene glycol]] (PEG-400, average of 9 EG units) utilizing the shake flask method - Valentine Anyiam
EXP294 Determination of the solubility of benzoic acid in ethylene glycol and diethylene glycol by mixing the solutions with a magnetic stirrer - Valentine Anyiam
EXP293 Determination of the solubility of benzoic acid in ethylene glycol by measuring exact concentrations with a volumetric flask - Valentine Anyiam
EXP292 Determination of the recrystallization yield of cinnamic acid in boiling n-hexane - Rida Atif
EXP291 Purify cinnamic acid through recrystallization from hexane and determine solubility via NMR of cinnamic acid in boiling hexane - Rida Atif
EXP290 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and [[#|polyethylene glycol]]. This experiment will also use the SAMS technique with a 2-chamber NMR tube to avoid solubility problems between CDCl3 and ethylene glycol polymers - Valentine Anyiam
EXP289 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and polyethylene glycol. This experiment will also use the SAMS technique with a 2-chamber NMR tube to avoid solubility problems between CDCl3 and ethylene glycol polymers - Valentine Anyiam
EXP288 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and polyethylene glycol. This experiment will also use the SAMS technique with a 2-chamber NMR tube to avoid solubility problems between CDCl3 and ethylene glycol polymers - Valentine Anyiam
EXP287 To determine the solubility of n-[(e)-(4-chlorophenyl)methylene]aniline in Hexane, ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol, and 6000 Poly(ethylene glycol) - Mark Mangir
EXP285 Determination of the solubility of cinnamic acid in boiling n-hexane to [[#|confirm]] results of EXP283 - Rida Atif
EXP284 Determination of the solubility of benzoic acid in ethylene glycol, diethylene glycol and glyme. -Valentine Anyiam
EXP283 Determination of the solubility of cinnamic acid boiling in n-hexane - Rida Atif
EXP282 Recrystallization of cinnamic acid in ethanol/water (50/50 volume).- Lizzie Clark
EXP281Recrystallization of cinnamic acid in n-hexane - Rida Atif
EXP280 Determination of solubility of cinnamic acid in methanol via the density method. -Rida Atif
EXP279 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone and recrystallization in ethyl acetate. -Matthew McBride
EXP278 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. -Matthew McBride
EXP277 Determination of solubility of cinnamic acid in ethylene glycol, diethylene glycol and dichloromethane. -Valentine Anyiam
EXP276 Recrystallization of cinnamic acid using hexane - Lacey Condron and Andrew Lang
EXP275 Determination of solubility of cinnamic acid in methanol via the density method. -Valentine Anyiam
EXP274 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. -Matthew McBride
EXP273 Recrystallization of cinnamic acid in pure ethanol. - Lizzie Clark
EXP272 To test the solubility of n-[(e)-(4-chlorophenyl)methylene]aniline in ethanol, acetonitrile, benzene, hexane, and THF by the SAMS NMR method.- Mark Mangir
EXP271 Recrystallization of cinnamic acid in ethanol/water. - Samantha Gaines
EXP270 Determination of the solubility of cinnamic acid in ethylene glycol and propanediol using HNMR method.-Stephanie Costa
EXP269 Formation of trans-dibenzalacetone from benzaldehyde and acetone. - Matthew McBride
EXP268 Determination of the solubility of cinnamic acid in ethylene glycol using the density method.-Stephanie Costa
EXP267 Determination of the solubility of 4-chlorobenzaldehyde in ethanol at room temperature (25C) Alex Greene
EXP266 Determination of the solubility of cinnamic acid in propylene glycol and glycerol using the density method. Unnati Hajari
EXP265 Determination of the solubility of cinnamic acid in methanol using the density method. Unnati Hajari
EXP264 Determination of the solubility of palmitic acid in 2-pentanol using the density method. - Ashley Sweeney
EXP263 Recrystallization of cinnamic acid in hexane. -Lacey Condron
EXP262 Recrystallization of cinnamic acid in distilled water.- Lizzie Clark
EXP261 Determination of the ratio of hemiacetal to 4-chlorobenzaldehyde in ethanol and methanol- Stephanie Costa
EXP260 Determination of the solubility of 4-chlorobenzaldehyde in ethanol and characterization of possible product using SAMS HNMR method. - Matthew McBride
EXP259 NMR of 4-chlorobenzaldehyde in ethanol to determine possible presence of other products- Alex Greene
EXP258 Determination of the solubility of 4-chlorobenzaldehyde in ethanol and methanol.- Stephanie Costa
EXP257 Determination of the solubility of palmitic acid in methanol using the density method. - Lizzie Clark
EXP256 Determination of the solubility of palmitic acid in 1-butanol using the density method - Lacey Condron
EXP255 Determination of the solubility of cinnamic acid in cyclohexanone and 1,2-dichloroethane by the SAMS NMR method. - Matthew McBride
EXP254 Determination of the solubility of palmitic acid in acetone using the density method - Lacey Condron
EXP253 Determination of the solubility of palmitic acid in 1-pentanol using the density method. - Lizzie Clark
EXP252 Determination of the solubility of cinnamic acid in nitromethane using the density method.- Stephanie Costa
EXP251 Determination of the solubility of trans-cinnamic acid in 1,2 dichloroethane using the density method. - Alex Greene
EXP250 Determination of the solubility of palmitic acid in 2-butanol using the density method. - Lizzie Clark
EXP249 Determination of the solubility of palmitic acid in 2-propanol using the density method. - Lacey Condron
EXP248 Determination of the solubility of palmitic acid in 1-propanol using the density method. - Lizzie Clark
EXP247 Determination of whether trans-cinnamic acid is miscible in a 5M solution of THF. - Matthew McBride
EXP246 Determination of the viability of trans-cinnamic acid at concentration 3M in THF - Alex Greene
EXP245 Determination of the solubility of trans-cinnamic acid in acetonitrile and THF using the density method. - Matthew McBride
EXP244 Determination of the solubility of trans-cinnamic acid in hexane - Stephanie Costa
EXP243 Determination of the solubility of cinnamic acid in DMSO and THF - Stephanie Costa
EXP242 Determination of the solubility of cinnamic acid in cyclohexane, DMSO, and THF - Stephanie Costa
EXP241 Determination of the solubility of cinnamic acid in 2-butanol - Lizzie, Lacey, Samantha
EXP240 Determination of the solubility of cinnamic acid in 2-propanol - Lacey, Lizzie, Samantha
EXP239 Determination of the solubility of cinnamic acid in 2-pentanol - Samantha, Lacey, Lizzie
EXP238 Determination of the solubility of cinnamic acid in chloroform.- Stephanie Costa
EXP237 Determination of the solubility of cinnamic acid in Methanol.- Stephanie Costa
EXP236 Determination of the solubility of trans-cinnamic acid in Benzene, Toluene, and Chloroform using the density method. - Matthew McBride
EXP235 Ugi synthesis experiment - moved to usefulchem wiki - Jenna Mancinelli
EXP234 Determination of the solubility of trans-cinnamic acid in acetone using the density method.- Lacey, Lizzie
EXP233 Determination of the solubility of trans-cinnamic acid in ethyl acetate using the density method.- Lacey, Lizzie
EXP232 Determination of the solubility of trans-cinnamic acid in propyl acetate using the density method.- Lizzie, Lacey
EXP231 Determination of the solubility of trans-cinnamic acid in Benzene, Toluene, and Chloroform using the density method. - Matthew McBride
Exp230 Determination of the solubility of benzoic acid, 4-chlorobenzoic acid and 2-phenylbutyric acid in 2,2,2-trifluoroethanol - Evan
EXP229 Determination of the solubility of Trans cinnamic acid in Methanol by the density method. - Matthew McBride
EXP228 Determination of the solubility of Trans cinnamic acid in Benzene, Toluene, Acetonitrile, and Trifluoroethanol by the SAMS NMR method.- Mark
EXP227 Determination of the solubility of Trans cinnamic acid in Ethanol and Methanol by the SAMS NMR method.- Mark
EXP226 Determination of the relative concentration of t-cinnamic acid in ethanol at different temperatures by density and NMR - Sozit
EXP225 Determination of the solubility of trans-cinnamic acid in 1-pentanol by density method - Samantha, Lizzie
EXP224 Determination of the solubility of trans-cinnamic acid in 1-octanol by density method - Lizzie, Samantha
EXP223 Determination of the solubility of trans-cinnamic acid in 1-butanol by density method - Samantha, Lacey, Lizzie
EXP222 Determination of the solubility of trans-cinnamic acid in 1-propanol by density method - Lizzie, Lacy, Samantha
EXP221 Determination of the solubility of trans-cinnamic acid in ethanol by density method - Lacey, Samantha, Lizzie
EXP220 Determination of the solubility of trans-cinnamic acid in methanol by density method - Samantha, Lacey, Lizzie
EXP219 Determination of the solubility of Trans cinnamic acid in Ethanol and Methanol by the SAMS NMR method.- Mark
Exp218 Determination of the solubility of trans-cinnamic aid, salicylic acid, p-dimethylaminobenzaldehyde and vanillin in trifluoroethanol by SAMS HNMR method- Evan
Exp217 Determination of the solubility of 5 imines in trifluoroethanol by SAMS HNMR method - Evan
Exp216 Determination of the solubility of 4 imines in 5 solvents. - Evan
Exp215 Determination of the solubility of benzalaniline in n-hexane, ethyl acetate, isopropanol, dichloromethane, and benzene by SAMS HNMR method - Evan
Exp214 Determination of the solubility of 4 imines in 90/10 ethanol/water mixture by SAMS HNMR method - Evan
Exp213 Determination of the solubility of benzalaniline in methanol by SAMS HNMR method - Evan
Exp212 Determination of solubility of benzalaniline in 5 solvents by SAMS HNMR method - Evan
Exp211 Determination of solubility of cinnamic acid in (several solvents) by density method - Mary
Exp210 Determination of solubility of 2-phenylbutyric acid in n-hexane by density method - Ha Pham
Exp209 Determination of solubility of cinnamic acid in ethanol by density method- Mary
Exp208 Determination of solubility of cinamic acid in methanol and ethanol by density method - Evan and Ha
Exp207 Determination of solubility of sample 1A from UCExp262 in toluene, acetonitrile, THF, and chloroform - Evan
Exp206 Determination of solubility of sample 1A from UCExp262 - Evan
Exp205 Determination of solubility of benzalaniline in 5 solvents - Evan
Exp204 Determination of solubility of 2-phenylbutyric acid in n-hexane by density method. - Evan
Exp203 Determination of solubility of 2-phenylbutyric acid in n-hexane, 2-propanol, and methanol by NMR. - Sozit
Exp202 Determination of solubility of trans-cinnamic acid in methanol using the density method. - John
Exp201 Determination of solubility of 2-phenylbutyric acid in methanol by density method. - Evan
Exp200 Determination of solubility of trans-cinnamic acid in methanol using the density method. - John
Exp199 Determination of solubility of Benzoic acid in chloroform, methanol and Hexane by density method. - Jianbo
Exp198 Determination of solubility of salicylic acid in chloroform, water and acetonitrile by density method. - Evan
Exp197 Determination of solubility of trans-cinnamic acid in methanol by density method. - Evan
Exp196 Determination of the concentration of Exp193-Sample3 by NMR and density methods. - Sozit
Exp195 Determination of the solubility of boc-alanine and boc-phenyl alanine in hexane, acetonitrile, methanol, t-butanol and benzene by the SAMS method- Khalid
Exp194 Determination of the solubility of boc-alanine and boc-phenyl alanine in hexane, acetonitrile, methanol, t-butanol and benzene by the SAMS method- Khalid
Exp193 Observation of solubility of 2-phenylbutyric acid in hexanes in different temperature(up to 45C) - Jianbo
Exp192 Determination of solubility of 2-phenylbutyric acid in three pure solvent ( benzene, methanol and hexene) at variable time in volumetric flasks-Jianbo
Exp191 Observation of solubility of benzaldehyde in n-hexane through melting point - Sozit
Exp190 Observation of solubility of t-butanol in n-hexane through melting point - Sozit
Exp189 Determination of solubility of piperonal in n-hexane at different temperatures using NMR - Sozit
Exp188 Observation of solubility of piperonal in hexanes through melting point - Jianbo
Exp187 Observation of solubility of piperonal in n-hexane in different temperature(up to 40C)- Jianbo
Exp186 Determination of solubility of piperonal in n-hexane using four sizes of volumetric flasks - Jianbo
Exp185 Observation of solubility of piperonal in n-hexane through melting point - Sozit
Exp184 Observation of solubility of cyclohexanecarboxylic acid in hexanes through melting point - Sozit
Exp183 Determination of solubility of cyclohexanecarboxylic acid in hexane at 25C and 0C - Jianbo
Exp182 statistically analyze the differences between methanol densities measured under different flask volumes- Wei
Exp181 Determination of error in different volumetric flasks using methanol and the density method - Jianbo
Exp180 Determination of error in different volumetric flasks using methanol and the density method - Sozit
Exp179 Determination of density of pure methanol in different flasks at room temperature - Jianbo
Exp178 Determination of solubility of different concentrations of cinnamic acid in methanol at room temperature - Sozit
Exp177 Determination of solubility of cinnamic acid in methanol at variable time in volumetric flasks-Jianbo
Exp176 Determination of solubility of cinnamic acid in methanol using four sizes of volumetric flasks - Sozit
Exp175 Determination of solubility of cinnamic acid in several solvents - Imran
Exp174 Determination of solubility of different solutes heated at variable times - Imran
Exp173 Verifying the density method of cinnamic acid in methanol using QCM - Imran
Exp172 Determination of the solubility of several solutes by density - Imran
Exp171 Determination of solubility of cinnamic acid in methanol - - Jessica
Exp170 Verifying the density method of cinnamic acid in methanol - Jessica
Exp169 Verifying the density method of cinnamic acid in methanol - Imran
Exp168 Verifying the density method of cinnamic acid in methanol - Jessica
Exp167 Determination of the solubility of Ugi 176C in EtOAc and phenanthrene-9-carboxaldehyde in THF - Khalid
Exp166 Effect of the three co-solutes on the solubility of the Ugi product UC176C in ethyl acetate - Khalid
Exp165
Determination the solubility of phenanthrene-9-carboxaldehyde, phenylacetic acid and the 176C(UC) in ethyl acetate by SAMS - Khalid
Exp164 Determination of the solubility of 2,6 dicholobenzaldephyde in DMSO and benzene using SAMS - Alisha
EXP163 Determination of the solubility of benzoic acid in absolute ethanol using density measurements- Harina
Exp162 Determination of the solubility of benzoic acid in methanol using density measurements - Alisha
Exp161 Determination of the solubility of Ugi 234 in ethanol by gravimetric analysis - David
Exp160 Determination of solubility of benzoic acid in ethanol by gravimetric analysis - David & Chau
Exp159 Estimation of the concentration of Ugi product (UC176C) left dissolved in a supernatant of its reaction - Khalid
Exp158 Effect of butylisocyanide concentration on the solubility of the Ugi product UC176C in benzene - Khalid & Hai
Exp157 Effect of phenylacetic acid concentration on the solubility of the Ugi product UC176C in benzene - Khalid
Exp156 Effect of imminium concentration on the solubility of the Ugi product UC176C in benzene - Khalid
Exp155 Determination of solubility of benzoic acid, phenylacetic acid and the Ugi product UC176C in 1-octanol - Khalid & Hai
Exp154 Effect of phenylacetic acid on the solubility of the Ugi product UCExp176C at lower concentration (0.01M - 0.5) in benzene - Hai & Khalid
Exp153 Effect of imminium concentration on the solubility of the Ugi product UC176C in methanol - Hai & Khalid
Exp152 Effect of imminium concentration on the solubility of the Ugi product UC176C in benzene - Hai & Khalid
Exp151 To measure the solubility of Ugi product UCExp176C in methanol with a) ~0.05 imine b) imine + phenylacetic acid. Hai & Khalid
Exp150 To measure the solubility of Ugi product UCExp176C in solution of benzene and a) phenanthrene-9-carboxaldheyde, furufylamine and phenylacetic acid as cosolutes Hai & Khalid
Exp149 To measure the solubility of Ugi product UCExp176C in 0.1M, 0.2M, 0.3M, 0.5M imine solution in benzene Hai & Khalid
Exp148 Determination of solubility of UC176C in a 0.1M imine solution in benzene b) 0.1M n-butylisocyanide solution in benzene - Hai & Khalid
Exp147
Effect of phenylacetic acid and fufurylamine (equimolar solutions) in benzene on the solubility of the Ugi product
UC176C - Khalid
Exp146 Effect of phenylacetic acid concentration on the solubility of the Ugi product UC176C in benzene - Khalid
Exp145 Determination of solubility of Ugi product UC148B in benzene, THF, acetonitrile, methanol and ethanol - Khalid & Hai
Exp144 Effect of starting materials on the solubility of Ugi product UC176C in benzene - Khalid & Hai
Exp143 Determination of solubility of boc-glycine in 2-propanol, benzene - Khalid & Hai
Exp142 Determination of solubility of salicylic acid in chloroform - Hai & Ciana
Exp141 Determination of solubility of salicylic acid in chloroform - Ciana
Exp140 Determination of solubility of salicylic acid in toluene - Ciana
Exp139 Determination of solubility of salicylic acid in toluene - Ciana
Exp138 Determination of the solubilities of four solutes in different solvents by NMR - Jenna Mancinelli
Exp137 Determination of the solubility of 4-acetamidobenzoic acid and nicotinic acid in five solvents - Khalid
Exp136 Determination of the solubilities of seven solutes in different solvents by NMR - Jenna Mancinelli
Exp135 Continuation of solubility-temperature study of Boc-Glycine in THF - Jenna Mancinelli
Exp134 Determination of solubility for Cbz-L-Proline in methanol - Khalid
Exp133 Determination of solubility-temperature curve for Boc-Glycine in THF - Jenna Mancinelli
Exp132 Determination of solubility of 3,4-(methylenedioxy)phenylacetic acid in methanol - Khalid
Exp131 Determination of solubility of 3,4-(methylenedioxy)phenylacetic acid in THF - Khalid
Exp130 Solubility-Temperature study of 4-nitrobenzaldehyde, Continued - Marshall Moritz
Exp129 Determination of solubility of 3,4-(methylenedioxy)phenylacetic acid in many solvents-Dan Rein
Exp128 Generation of solubility-temperature curve for 4-nitrobenzaldehyde in four solvent mixture - Jenna Mancinelli
Exp127 Compound 237-1B (176C) solubility in different sovents at 23 degrees C.- Anthony Shorrock
Exp126 DOSOL Temperature study of benzoic acid in methanol-Dan Rein
Exp125 DOSOL Determination of solubility of Ugi product UCExp235-2A in different solvents by NMR- Khalid, Jenna
Exp124 DOSOL Temperature study of 3,4 methylenedioxyphenylacetic acid in acetonitrile- Matthew Federici
Exp123 Determination of solubility of phenylacetic acid in 4 different solvents by NMR and recrystallization methods - Marshall Moritz
Exp122 Solubility-Temperature study of 4-nitrobenzaldehyde, Continued - Marshall Moritz
Exp121 Temperature study of 4-fluorobenzoic acid in ethanol-Dan Rein
Exp120 Temperature study of 4-fluorobenzoic acid in ethanol- Dan Rein
Exp119 Temperature study of 3,4 methylenedioxyphenylacetic acid in methanol- Matthew Federici
Exp118 DOSOL Temperature study of benzoic acid in methanol - Anthony Shorrock
Exp117 DOSOL Temperature study of BOC-Glycine and THF at specific concentrations-Daniel Rein
Exp116 Temperature study of BOC-Glycine and THF-Daniel Rein
Exp115 Verification of the SAMS using varying concentrations of benzoic acid in DMF - David
Exp114 Constucting a solubility curve for 4-nitrobenzaldehyde in a 4-solvent system - Marshall Moritz
Exp113 Determination of solubility of Ugi product UCExp216-3A in different solvents by NMR- Jenna
Exp112 Generating a solubility-temperature curve of pyrene in acetonitrile - Jenna
Exp111 Generating a solubility-temperature curve for 4-nitrobenzaldehyde in acetonitrile and chloroform by recrystallization - Marshall Moritz
Exp110 Generating a solubility-temperature curve for 4-nitrobenzaldehyde in methanol by recrystallization - Marshall Moritz
Exp109 Construction of a solubility curve for pyrene in acetonitrile by cooling crystallization method - Khalid, Dr. Bradley, Cedric
Exp108 Determination of the solubility of pyrene in acetonitrile - Marshall Moritz
Exp107 Determination of the solubility of p-toluenesulfonic acid in toluene and acetonitrile - Marshall Moritz
Exp106 Determination of the solubility of p-Fluorobenzoic acid in six different solvents - Marshall Moritz
Exp105 Determination of the solubility of 2-chloro-5-nitrobenzaldehyde in six different solvents - Marshall Moritz
Exp104 Determination of the solubility of furoic acid in five different solvents - Marshall Moritz
Exp103 Verification of the SAMS method using varying concentrations of 1-pyrenebutyric acid in different solvents - Khalid
Exp102 Verification of the SAMS method using varying concentrations of 2-phenylbutyric acid in DMSO - David
Exp101 Determination of 0.6 M solution of 4-pyrenebutanoic acid in 0.4347:1.000 solution of THF:ethanol - David
Exp100 Determination of the solubility of nicotinic acid in 5 different solvents - Marshall Moritz
Exp099 Determination of the solubility of 4-pyrenebutanoic acid in DMF and DMSO - David
Exp098 DOSOL Determination of the solubility of eight solutes in methanol, acetonitrile, and DMSO - Matthew Federici
Exp097 Determination of the solubility of Ugi product 216-4A in 5 different solvents - Matthew Federici
Exp096 Determination of the solubility of Ugi product 216-7A in 6 different solvents - David
Exp095 Determination of the solubility of chloroacetic acid in 5 different solvent - Marshall Moritz
Exp094 Verification of the SAMS method using a 2.81 M solution of 2-phenylbutyric acid in THF - David
Exp093 Determination of the solubility of Ugi product 216-4A in methanol, ethanol, and acetonitrile- Cedric
Exp092 Determination of the solubility of 4-methoxyphenylacetic acid in THF (verification) - David
Exp091 Determination of the solubility of 4-pyrenebutanoic acid in THF (verification) - David
Exp090 Determination of the solubility of 2,3-Dihydroxybenzoic acid in 6 different solvents- Shuba
Exp089 Determination of the solubility of 4-methoxyphenylacetic acid in 5 different solvents - Marshall Moritz
Exp088 Determination of the solubility of 4-hydroxybenzaldehyde in THF - Marshall Moritz
Exp087 Determination of solubility of 2,4,6-Trihydroxybenzoic acid in 6 different solvents- Shuba
Exp086 Determination of the solubility of phenylacetic acid in acetonitrile and toluene- Cedric
Exp085 Determination of the solubility of six solutes in THF - Matthew Federici
Exp084 Determination of the solubility of 4-pyrenebutanoic acid in THF (verification) Khalid
Exp083 Determination of the solubility of 2-phenylbutyric acid in toluene, THF, and DMSO by NMR spectroscopy- Cedric
Exp082 Determination of the solubility of six solutes in THF - Matthew Federici
Exp081 Determination of the solubility of dipheylacetic acid in six solvents - Khalid, Shuba
Exp080 Determination of the solubility of 2-phenylbutyric acid in DMSO, THF, and toluene- Cedric
Exp079 Determination of the solubility of 2-phenylbutyric acid in ethanol and acetonitrile by NMR spectroscopy- Cedric
Exp078 Determination of the solubility of one Ugi product in six solvents - Matthew Federici
Exp077 Determination of the solubility of Diphenylacetic acid in methanol - Matthew Federici
Exp076
Determination of the solubility of two Ugi products in six solvents - Shuba, Khalid
Exp075 Determination of the solubility of 4-chlorophenylacetic acid in seven solvents - Shuba, Khalid
Exp074
(DOSOL) Determination of the solubility of 4-pyrenebutanoic acid in THF and a 3:1 mix of THF and methanol - Khalid
Exp073 Determination of the solubility of 4-chlorophenylacetic acid in methanol and THF using 2 methodologies by NMR- Cedric
Exp072 Determination of the solubility of DL-mandelic acid, trans-cinnamic acid, 4-phenylbutyric acid, L-ascorbic acid, acetylsalicylic acid and 4,4-azoxydibenzoic acid in various solvents using 1H NMR - David

Exp071
Determination of the solubility of the Ugi product UC215C, vertatraldehyde, piperonal and Boc-glycine in different solvents - Khalid
Exp070 (DOSOL) Determination of the solubility of Octadecylamine and 5 solvents - HaeJi
Exp069 Determination of the solubility of Octadecylamine and 5 solvents - HaeJi
Exp068 (DOSOL) Determination of the solubility of TOSMIC and octadecylamine in acetonitrile - Khalid
Exp067 Verifying the concentrations of 0.25M
4-pyrenebutanoic acid
solution and 1.25M crotonic acid solution in DMSO by HNMR- Khalid, Cedric
EXP066 JennyHale-16: Measuring the solubility of 8-bromo-octanoic acid in ethanol - Jenny
Exp065 Determination of the solubility of eleven Ugi products in methanol by HNMR - Khalid
Exp064 Determination of the solubility of crotonic acid in acetonitrile, chloroform, ether, DMSO, and n-hexane by NMR -Cedric
EXP063 JennyHale-15: Measuring the solubility of the liquid aldehydes 3,5-dimethylbenzaldehyde and 4-ethylbenzaldehyde in ethanol, methanol and THF by miscibility and density calculations. - Jenny
Exp062 Determination of the solubility of crotonic acid in methanol, THF, benzene, ethanol, and toluene by NMR -Cedric
Exp061 Determination of the solubility of the 4-pyrenebutanoic acid sixteen solvents - Khalid
Exp060 Determination of the solubility of the phenanthrene-9-carboxaldehyde in sixteen solvents - Khalid
EXP059 JennyHale-14 : Measuring the solubility of liquid aldehyde 3,4-dimethylbenzaldehyde in ethanol, methanol and THF - Jenny
EXP058 JennyHale-13: Measuring the solubilities of benzoic acid and undecanoic acid in ethanol, methanol and THF. Re-measuring the solubility of 4-hydroxybenzaldehyde in THF. - Jenny
EXP057 JennyHale-12: Measuring the solubilities of 10-chloro-9-anthraldehyde; 4-hydroxybenzaldehyde and 4-hydroxy-3-methylbenzaldehyde in ethanol, methanol and THF - Jenny
Exp056 Determination of the solubility of the Ugi product UC206B in seventeen solvents - Khalid
Exp055 Determination of the solubility of Vanillin in Ethanol - DU students
Exp054 Determination of the solubility of Succinic Acid in Ethanol - DU students
Exp053 Determination of the solubility of Urea in Methanol - DU students
Exp052 Determination of the solubility of Salicylic Acid in Methanol - DU students
Exp051 Determination of the solubility of Phenanthrene-9-carboxaldehyde & 1-pyrenebutyric acid in DMSO by NMR - Khalid
Exp050 Determination of the solubility of Vanillin in Ethanol - DU students
Exp049 Determination of the solubility of Citric Acid Monohydrate in Water - DU students
Exp048 Determination of the solubility of Cinnamic Acid in Methanol - DU students
Exp047 Determination of the solubility of Phthalic Acid in Methanol - DU students
Exp046 Determination of the solubility of Riboflavin in Methanol - DU students
Exp045 Determination of the solubility of Succinic Acid in Isopropanol - DU students
Exp044 Determination of the solubility of Succinic Acid in Ethanol - DU students
Exp043 Determination of the solubility of Benzoic Acid in Methanol - DU students
Exp042 Determination of the solubility of Succinic Acid in Ethanol - DU students
Exp041 Determination of the solubility of 3,4-Dimethoxybenzaldehyde in Acetone - DU students
Exp040 Determination of the solubility of Maleic Acid in Methanol - DU students
Exp039 Determination of the solubility of Maleic Acid in Ethanol - DU students
Exp038 Determination of the solubility of Tartaric Acid in Acetone - DU students
Exp037 Determination of the solubility of Benzoic Acid in Acetone - DU students
Exp036 Determination of the solubility of Salicylic Acid in Ethanol - DU students
Exp035 Determination of the solubility of Acetanilide in Acetone - DU students
EXP034 Determination of solubility of salicylic acid, acetylsalicylic acid, and o-anisic acid in protonated chloroform. - David
Exp033 Determination of solubility of
veratraldehyde
,
4-dimethylaminobenzaldehyde
, 4-chlorobenzaldehyde, 2,6-dichlorobenzaldehyde, 2-chloro-3-nitro-benzaldehyde and 4-nitrobenzaldehyde in methanol. - Cedric & Khalid
EXP032 (JennyHale-11) Repeat of JennyHale-3: Measuring the solubilities of benzotriazole-5-carboxylic acid; 8-bromooctanoic acid; 4-dimethylaminocinnamaldehyde and 2-(4-hydroxyphenyl)azobenzoic acid in ethanol and methanol. - Jenny
EXP031 Confirming the solubility of Benzoic acid in Chloroform using 1H NMR - David
EXP030 Determination of solubility of Phenanthrene-9-carboxaldehyde, 1-pyrenebutyric acid and piperonal in different solvents by NMR- Khalid
Exp029 Determining the solubility of Octylamine, Cyclohexylamine, Benzylamine, Aniline, and o-Chloroaniline in Methanol using different combination analysis -Cedric
EXP028 Proton NMR Integral Ratio Comparision using 4-Chlorobenzaldehyde in Chloroform-d - David

Exp027
Determination of solubility of Phenanthrene-9-carboxaldehyde in methanol by NMR- Khalid
Exp026 Determining the solubility of Furfurylamine and 5-Methyl-2-Furanmethanamine in Methanol using different combination analysis -Cedric

EXP025 (JennyHale-10) Repeat of JennyHale-2: Measuring the solubilities of citric acid, 2-oxoglutaric acid, sinapic acid and p-Toluic acid in ethanol, methanol and THF - Jenny

Exp024
Determination of solubility of Phenanthrene-9-carboxaldehyde and 1-Pyrenebutyric acid in methanol by UV-Vis - Khalid
Exp023 Determination of solubility of 2-naphthaldehyde, 4-hydroxybenzaldehyde, 4-nitrobenzaldehyde, o-vanillin and piperonal in methanol by UV-Vis -Khalid
Exp022 Determination of solubility of 19 liquid carboxylic acids and 2 aldehyes in methanol -Khalid
Exp021 Determination of solubility of fourteen liquid aldehydes in methanol -Khalid
Exp020 Determination of solubility of 2-furaldehyde in methanol -Khalid
Exp019 Determination of solubility of vanillin in methanol by UV-Vis -Khalid
Exp018 Determination of extinction coefficient of vanillin in methanol (UV) - Khalid
EXP017 Solubility determination procedure for 4-chlorobenzaldehyde in non-deuterated chloroform by proton NMR using sonicator- David
EXP016 Solubility determination procedure for 4-chlorobenzaldehyde in non-deuterated chloroform by proton NMR - David
EXP015 (JennyHale-9) Measuring the solubility of 4-hydroxyphenylpyruvic acid, 11-mercapto-undecanoic acid and 4-nitrophenylacetic acid in ethanol and methanol - Jenny
EXP014 (JennyHale-8) Measuring the solubility of 1-adamantylamine and 6-aminocaproic acid in ethanol and methanol - Jenny
EXP013 (JennyHale-7) Study of Temperature effect on solubility of vanillin in methanol and ethanol 3 - Jenny
EXP012 Determining the extinction coefficient of 4-chloroenzaldehyde via UV/VIS.- Tim
EXP011 (JennyHale-6) Study of Prolonged Vortexing time solubility of vanillin in methanol and ethanol - Jenny
EXP010 (JennyHale-5) Study of Temperature effect on solubility of vanillin in methanol and ethanol 2 - Jenny
EXP009 Solubility of benzoic acid in toluene- Cedric
EXP008 (JennyHale4) Study of Temperature effect on solubility of vanillin in methanol and ethanol - Jenny
EXP007 Solubility of benzoic acid and 4-chlorobenzoic acid in varying solvents.- Tim
EXP006 Solubility of 4-chlorobenzaldehyde in chloroform and methanol by UV spectroscpy - Khalid
EXP005 Solubility of benzoic acid in methanol - Cedric
EXP004 Speedvac on phenanthrene-9-carboxaldehyde, 4-chlorophenylacetic acid, and vanillin- Tim
EXP003 (JennyHale 3) - Jenny
EXP002 (JennyHale-2) - Jenny
EXP001 (JennyHale-1) - Jenny

List of Solubility Experiments on UsefulChem

UC-EXP212 (Tim Bohinski) speedvac on 4-nitrobenzaldehyde
UC-EXP211 (Khalid Mirza) UV on 4-chlorobenzaldehyde
UC-EXP210 (Khalid Mirza)
UC-EXP209 (Khalid Mirza and Tim Bohinski)
UC-EXP208 (Khalid Mirza and Tim Bohinski)
UC-EXP207 (Jean-Claude Bradley and Cameron Neylon)
UC-EXP205 (Khalid Mirza and Tim Bohinski)

Researcher

Alex Greene

Objective

To determine if trans-cinnamic acid can be made into a 3.0 M concentration in the solvent THF using a 5ml volumetric flask

Procedure

Cinnamic acid was measured to on a balance to have a concentration of 3M in a 5ml volumetric flask. The Cinnamic acid was added to a volumetric flask. Then THF was added to the flask up to the 5ml mark on the volumetric flask.

Results

The Cinnamic acid failed to completely dissolve in the THF at room temperature with mixing by inverting and sonication. Undissolved cinnamic acid remained at the bottom of the volumetric flask.

Discussion

Conclusion

The Cinnamic acid failed to completely dissolve in the solution of THF. The result is a contradiction of EXP 245, which had a cinnamic acid concentration around 3M

Log

2012-01-11

11:17- A 5ml volumetric flask was weight at 23.7969g
11:20- 2.2260g of trans-cinnamic acid was weighted and transferred to volumetric flask
11:28- THF was added to volumetric flask up to 5ml mark
11:34- Inverted flask repeatedly for 8 seconds to mix solution
11:35- Sonicated flask for 5 seconds
11:38- Took picture #1