MatthewMcBride

=Experiments Conducted by [|Matthew McBride]=

Experiments listed in the [|Reaction Attempts Database] [|Recrystallization SmartPhone Application] for choosing a recrystallization solvent of an organic compound

Research Reports: Winter Quarter 2013 Spring Quarter 2013 [|Fall Quarter 2013]

Experiments Listed Under ONSchallenge
EXP359 Recrystallization of benzoic acid from water with a pentane wash using the sintered glass funnel method. - **Matthew McBride** EXP358 Recrystallization of caffeine from toluene with a pentane wash using the sintered glass funnel method. - **Matthew McBride** EXP355 Examination of the ability of pentane to wash 1:1 ethanol/water(vol) from trans-cinnamic acid crystals. - **Matthew McBride** EXP354 Examination of layer separation of water in the ethanol/pentane binary solvent system. - **Matthew McBride** EXP353 Recrystallization of trans-dibenzalacetone from ethanol using the sintered glass funnel method. - **Matthew McBride** EXP352 Recrystallization of trans-cinnamic acid from cyclohexane using the sintered glass funnel method. - **Matthew McBride** EXP351 Recrystallization of benzoic acid from n-hexane using the sintered glass funnel method. - **Matthew McBride** EXP346 Recrystallization of caffeine from 1-octanol and washing with pentane at 1.0M concentration using the sintered glass funnel method. - **Matthew McBride** EXP343 Recrystallization of caffeine from 1-octanol and washing with pentane at 1.5M, 0.75M and 0.25M concentrations using the centrifuge method. - **Matthew McBride** EXP342 Recrystallization of caffeine from 1-octanol and washing with pentane at 2.0M, 0.75M and 0.25M concentrations. - **Matthew McBride** EXP338 Determination of the solubility of phenanthrene-9-carboxaldehyde in ethyl acetate and benzene by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP337 Determination of the solubility of phenanthrene-9-carboxaldehyde in THF and methanol by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP336 Determination of the solubility of trans-dibenzalacetone in water and 1-octanol at 25°C using UV/Vis Spectroscopy and the Shake Flask Method. - **Matthew McBride** EXP335 Determination of the LogP of trans-dibenzalacetone using 10% and 1% saturated 1-octanol in pure water. - **Matthew McBride** EXP333 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP332 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP331 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP329 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP328 Determination of the solubility of trans-dibenzalacetone in water and 1-octanol at 25°C using UV/Vis Spectroscopy and the Shake Flask Method. - **Matthew McBride** EXP325 Determination of the recrystallization yield of trans-dibenzalacetone in n-hexane. - **Matthew McBride** EXP324 Determination of the solubility of trans-dibenzalacetone in n-hexane, cyclohexane, methanol, 2-propanol and an ethanol/water mixture (50:50vol) by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP323 Determination of room temperature solubility of benzoic acid in ethanol/water mixtures of 40:60, 50:50, 60:40 volumes as well as pure ethanol, and trans-dibenzalacetone in pure ethanol - **Rida Atif and Matthew McBride** EXP322 Determination of the recrystallization yield of trans-dibenzalacetone in ethanol/water (50:50vol). - **Matthew McBride** EXP321 Determination of the recrystallization yield of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP314 Synthesis of trans-dibenzalacetone from acetone and benzaldehyde in an ethanol solvent and purifying by recrystallization from ethanol. - **Matthew McBride** EXP313 Determination of the solubility of trans-dibenzalacetone in diethyl ether and acetone by SAMS HNMR using the shake flask method to dissolve. - **Matthew McBride** EXP311 Determination of the solubility of trans-dibenzalacetone in methanol, cyclohexanol, and acetonitrile by SAMS HNMR using the shake flask method to dissolve. - **Matthew McBride** EXP308 Determine the solubility of benzene, THF, Cyclohexane, Cyclohexanone and Toluene by SAMS NMR using the Shake Flate method to dissolve. - **Matthew McBride** EXP307 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. - **Matthew McBride** EXP302 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. - **Matthew McBride** EXP301 Determination of the solubility of trans-dibenzalacetone in ethyl acetate, ethanol, and hexanes by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP300 Purification of trans-dibenzalacetone by recrystallization from ethanol. - **Matthew McBride** EXP279 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone and recrystallization in ethyl acetate. -**Matthew McBride** EXP278 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. -**Matthew McBride** EXP274 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. -**Matthew McBride** EXP269 Formation of trans-dibenzalacetone from benzaldehyde and acetone. - **Matthew McBride** EXP260 Determination of the solubility of 4-chlorobenzaldehyde in ethanol and characterization of possible product using SAMS HNMR method. - **Matthew McBride** EXP255 Determination of the solubility of cinnamic acid in cyclohexanone and 1,2-dichloroethane by the SAMS NMR method. - **Matthew McBride** EXP247 Determination of whether trans-cinnamic acid is miscible in a 5M solution of THF. - **Matthew McBride** EXP245 Determination of the solubility of trans-cinnamic acid in acetonitrile and THF using the density method. - **Matthew McBride** EXP236 Determination of the solubility of trans-cinnamic acid in Benzene, Toluene, and Chloroform using the density method. - **Matthew McBride** EXP231 Determination of the solubility of trans-cinnamic acid in Benzene, Toluene, and Chloroform using the density method. - **Matthew McBride** EXP229 Determination of the solubility of Trans cinnamic acid in Methanol by the density method. - **Matthew McBride**

Experiments Listed Under UsefulChem
EXP286 Synthesis of aldol condensation product of phenanthrene-9-carboxaldehyde and acetone in methanol using NaOH as the catalyst. -**Matthew McBride** EXP285 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as the catalyst. - **Matthew McBride** EXP284 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as the catalyst. - **Matthew McBride** EXP283 Synthesis of trans-dibenzalacetone in ethanol using piperidine as catalyst. - **Matthew McBride** EXP282 Synthesis of trans-dibenzalacetone in ethanol/water (1:1 vol) using NaOH as catalyst. - **Matthew McBride** EXP281 Synthesis of trans-dibenzalacetone in ethanol using piperidine as catalyst. - **Matthew McBride**

Experiments Listed Under Chemical Rediscovery Survey
CRSEXP027 Acetone and piperidine - **Matthew McBride** CRSEXP029 D2O HNMR shift using the coaxial NMR tube system. - **Matthew McBride** CRSEXP032 Acetone, Ethanol, Methanol and D2O HNMR shift using the coaxial NMR tube system with D2O and CDCl3 as the reference solvents. - **Matthew McBride** CRSEXP035 Salicylaldehyde and Ethanol, Methanol, Benzene and Propylamine. - **Matthew McBride**