Exp213

=Researcher= Evan Curtin =Objective= To determine the solubility of benzalaniline in methanol via sams HNMR method in order to be able to predict the solubility in 72 solvents. =Procedure= =Results= SAMS Spreadsheet media type="custom" key="9838423" =Discussion= =Conclusion= The solubility of benzalaniline in methanol is 1.48M. =Log=
 * [referring to the objective - were there any surprises in the solubility predictions based on the calculated Abraham descriptors? JCB]**

2011-06-20
12:26 - Mixed benzalaniline and methanol in a 1-dram vial. Turned on heating bath (RT is 24C) 12:42 - Added mixture to bath, temperature 36C 12:44 - Mixture dissolved completely, removed from bath. 12:53 - Blew air on solution for roughly 30 seconds, precipitate started to form. Let sit on counter, with cap on.

14:10 - Removed supernatant from the mixture (roughly 150-250 micro liters). Added CDCl3. Put sample in NMR tube. 14:30 - Took HNMR using 300 MHz varian NMR.
 * 2011-06-21**