ONSCExp080


 * Exp081[Don't put ONSC when you make new experiment pages JCB]**

To estimate the solubility of the Ugi produts UC216-2A and UC216-5A by NMR.
 * Objective**


 * Procedure

Results

Log 2009-04-13** 1:15 Labeled 6 half-dram vials from 1-6. 1:20 Placed a small amount of the solute (UC216-2A)in each vial. 1:25 Pipetted out 200uL of the six primary solvents into the vials;namely..methanol Vial **#1**, ethanol-Vial **#2,** acetonitrile-Vial **#3,** toulene-Vial **#4,**THF-vial **#5,** and DMSO-vial **#6.** 1:30 Placed the vials in the sonicator, temperature recorded was 24C. 1:50 Vials were removed form the sonicator. 1:55 Labeled 6 of half-dram vials from A-F and filled them with small amount of the solute (UC216-5A). 1:57 Pipetted out 200uL of the six primary solvents to the vials...methanol Vial **#1**, ethanol-Vial **#2**, acetonitrile-Vial **#3**, toluene-Vial **#4**, THF-vial **#**5**,** and DMSO -vial **#6.** 2:00 Placed the vials A-F in the sonicator and the temperature recorded was 29C. 2:20 The vials were removed form the sonicator.