List+of+Experiments



**Summary Solubility Data (CC0)** [|SolubilitiesSum Spreadsheet] **(****Read these instruction before adding data****)** ([|Chemicalize version] - hover over names to view structures) [|SolSumMix] (for mixtures and temperatures) [|Request an Experiment] (Andrew Lang) [|Web Query Interface (Rajarshi Guha)] [|Alternate Solubility Web Query Interface That Accepts GET Queries] (Andrew Lang) [|More Web Services] (Pierre Lindenbaum and Egon Willighagen) [|Visualizing Chemical Space] (Rajarshi Guha) [|PCA Chemical Space] (Andrew Lang) [|CDK Descriptor Chemical Space] (Andrew Lang) [|Solubility Prediction] (Rajarshi Guha) [|List a summary of all measurements for a solute in a table via simple URL]([|XML version]) (Andrew Lang) [|List of all solutes with their SMILES, CSID and hyperlink] (Andrew Lang) [|ONS solubility challenge as a data source in ChemSpider] - [|see description] (Tony __Williams__) [|Summary of all measurements] (Andrew Lang) [|Outliers] (Andrew Lang) [|ONSgrid checklist] =List of Experiments on this wiki= EXP359 Recrystallization of benzoic acid from water with a pentane wash using the sintered glass funnel method. - **Matthew McBride** EXP358 Recrystallization of caffeine from toluene with a pentane wash using the sintered glass funnel method. - **Matthew McBride** EXP357 Measurement of the solubility of Cinnamic acid in 10% ethanol in pentane. - **Ene Anteyi** EXP355 Examination of the ability of pentane to wash 1:1 ethanol/water(vol) from trans-cinnamic acid crystals. - **Matthew McBride** EXP354 Examination of layer separation of water in the ethanol/pentane binary solvent system. - **Matthew McBride** EXP353 Recrystallization of trans-dibenzalacetone from ethanol using the sintered glass funnel method. - **Matthew McBride** EXP352 Recrystallization of trans-cinnamic acid from cyclohexane using the sintered glass funnel method. - **Matthew McBride** EXP351 Recrystallization of benzoic acid from n-hexane using the sintered glass funnel method. - **Matthew McBride** EXP350 Recrystallization of trans-cinnamic acid from 1:1 ethanol/water(vol) and washing with pentane using the sintered glass funnel method. - **Rani Saba** EXP349 Recrystallization of caffeine with 10% trans-cinnamic acid impurity from 1-octanol and washing with pentane at 0.75M concentration using the heat gun and a test tube with the sintered glass funnel method. - **Unnati Hajari** EXP348 Recrystallization of caffeine with 50% trans-cinnamic acid impurity from 1-octanol and washing with pentane at 0.75M concentration using the heat gun and a test tube with the sintered glass funnel method. - **Rani Saba** EXP347 Recrystallization of caffeine from 1-octanol and washing with pentane at 0.75M concentration using the heat gun and a test tube with the sintered glass funnel method. - **Paris Dayon Favors II** EXP346 Recrystallization of caffeine from 1-octanol and washing with pentane at 1.0M concentration using the sintered glass funnel method. - **Matthew McBride** EXP345 Recrystallization of salicylic acid in 1-octanol using pentane to wash the crystals. - **Hieu Nguyen** EXP344 Recrystallization of trans-cinnamic acid from 1-octanol and washing with pentane at 1.5M, 0.75M and 0.25M concentrations using the centrifuge method. - **Rani Saba** EXP343 Recrystallization of caffeine from 1-octanol and washing with pentane at 1.5M, 0.75M and 0.25M concentrations using the centrifuge method. - **Matthew McBride** EXP342 Recrystallization of caffeine from 1-octanol and washing with pentane at 2.0M, 0.75M and 0.25M concentrations. - **Matthew McBride** EXP341 Determination of the solubility of phenanthrene-9-carboxaldehyde in chloroform by the SAMS HNMR method using the shake flask method to dissolve. - **Hieu Nguyen** EXP340 Determination of the solubility of trans-cinnamic acid in methanol by using the density method. - **Linh Bui** EXP339 Determination of the solubility of trans-cinnamic acid in methanol by using the density method. - **Hieu Nguyen** EXP338 Determination of the solubility of phenanthrene-9-carboxaldehyde in ethyl acetate and benzene by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP337 Determination of the solubility of phenanthrene-9-carboxaldehyde in THF and methanol by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP336 Determination of the solubility of trans-dibenzalacetone in water and 1-octanol at 25°C using UV/Vis Spectroscopy and the Shake Flask Method. - **Matthew McBride** EXP335 Determination of the LogP of trans-dibenzalacetone using 10% and 1% saturated 1-octanol in pure water. - **Matthew McBride** EXP334 Determination of room temperature solubility of cinnamic acid in water, octanol, hexane, and cyclohexane - **Rida Atif** EXP333 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP332 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP331 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP330 Determination of room temperature solubility of cinnamic acid in hexane and cyclohexane - **Rida Atif** EXP329 Determination of the extinction coefficient of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP328 Determination of the solubility of trans-dibenzalacetone in water and 1-octanol at 25°C using UV/Vis Spectroscopy and the Shake Flask Method. - **Matthew McBride** EXP327 Determination of room temperature solubility of benzoic acid in ethanol/water 30:70 volume - **Rida Atif** EXP326 Determination of room temperature solubility of benzoic acid in ethanol/water mixtures of 30:70, 40:60, and 50:50 volumes - **Rida Atif** EXP325 Determination of the recrystallization yield of trans-dibenzalacetone in n-hexane. - **Matthew McBride** EXP324 Determination of the solubility of trans-dibenzalacetone in n-hexane, cyclohexane, methanol, 2-propanol and an ethanol/water mixture (50:50vol) by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP323 Determination of room temperature solubility of benzoic acid in ethanol/water mixtures of 40:60, 50:50, 60:40 volumes as well as pure ethanol, and trans-dibenzalacetone in pure ethanol - **Rida Atif and Matthew McBride** EXP322 Determination of the recrystallization yield of trans-dibenzalacetone in ethanol/water (50:50vol). - **Matthew McBride** EXP321 Determination of the recrystallization yield of trans-dibenzalacetone in ethanol. - **Matthew McBride** EXP320 Determination of the solubility at room temperature of benzoic acid in ethanol/water(40:60) - **Rida Atif** EXP319 Determination of the recrystallization yield of benzoic acid in ethanol/water(12:20) - **Rida Atif** EXP318 Determination of the recrystallization yield of benzoic acid in ethanol/water(40:60)vol - **Rida Atif** EXP317 Determination of the recrystallization yield of benzoic acid in ethanol/water(12:20) - **Rida Atif** EXP316 Determination of the recrystallization yield of cinnamic acid in carbon tetrachloride - **Rida Atif** EXP315 Determination of the recrystallization yield of benzoic acid in carbon tetrachloride - **Rida Atif** EXP314 Synthesis of trans-dibenzalacetone from acetone and benzaldehyde in an ethanol solvent and purifying by recrystallization from ethanol. - **Matthew McBride** EXP313 Determination of the solubility of trans-dibenzalacetone in diethyl ether and acetone by SAMS HNMR using the shake flask method to dissolve. - **Matthew McBride** EXP312 Determination of the recrystallization yield of cinnamic acid in benzene - **Rida Atif** EXP311 Determination of the solubility of trans-dibenzalacetone in methanol, cyclohexanol, and acetonitrile by SAMS HNMR using the shake flask method to dissolve. - **Matthew McBride** EXP310 Determination of the recrystallization yield of cinnamic acid in n-hexane - **Rida Atif** EXP309 Determination of the recrystallization yield of cinnamic acid in cyclohexane - **Rida Atif** EXP308 Determine the solubility of benzene, THF, Cyclohexane, Cyclohexanone and Toluene by SAMS NMR using the Shake Flate method to dissolve. - **Matthew McBride** EXP307 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. - **Matthew McBride** EXP306 Determination of the recrystallization yield of benzoic acid in hexane - **Rida Atif** EXP305 Determination of the recrystallization yield of benzoic acid in cyclohexane - **Rida Atif** EXP304 Determination of the recrystallization yield of benzoic acid in ethanol/water (40:60) - **Rida Atif** EXP303 Determination of the recrystallization yield of benzoic acid in benzene - **Rida Atif** EXP302 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. - **Matthew McBride** EXP301 Determination of the solubility of trans-dibenzalacetone in ethyl acetate, ethanol, and hexanes by the SAMS HNMR method using the shake flask method to dissolve. - **Matthew McBride** EXP300 Purification of trans-dibenzalacetone by recrystallization from ethanol. - **Matthew McBride** EXP299 Determination of the recrystallization yield of benzoic acid in benzene - **Rida Atif** EXP298 Determination of the recrystallization yield of benzoic acid in benzene - **Rida Atif** EXP297 Determine the solubility of n-[(e)-(4-chlorophenyl)methylene]aniline in ethanol, acetonitrile, benzene, hexane, and THF by the SAMS NMR method, dissolved using shake plate method. - **Mark Mangir** EXP296 Determination of the solubility of cinnamic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and __#|polyethylene glycol__ (PEG-400, average of 9 EG units) utilizing the shake flask method - **Valentine Anyiam** EXP295 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and __#|polyethylene glycol__ (PEG-400, average of 9 EG units) utilizing the shake flask method - **Valentine Anyiam** EXP294 Determination of the solubility of benzoic acid in ethylene glycol and diethylene glycol by mixing the solutions with a magnetic stirrer - **Valentine Anyiam** EXP293 Determination of the solubility of benzoic acid in ethylene glycol by measuring exact concentrations with a volumetric flask - **Valentine Anyiam** EXP292 Determination of the recrystallization yield of cinnamic acid in boiling n-hexane - **Rida Atif** EXP291 Purify cinnamic acid through recrystallization from hexane and determine solubility via NMR of cinnamic acid in boiling hexane - **Rida Atif** EXP290 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and __#|polyethylene glycol__. This experiment will also use the SAMS technique with a 2-chamber NMR tube to avoid solubility problems between CDCl3 and ethylene glycol polymers - **Valentine Anyiam** EXP289 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and polyethylene glycol. This experiment will also use the SAMS technique with a 2-chamber NMR tube to avoid solubility problems between CDCl3 and ethylene glycol polymers - **Valentine** **Anyiam** EXP288 Determination of the solubility of benzoic acid in a series of glycol solvents: ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol and polyethylene glycol. This experiment will also use the SAMS technique with a 2-chamber NMR tube to avoid solubility problems between CDCl3 and ethylene glycol polymers - **Valentine** **Anyiam** EXP287 To determine the solubility of n-[(e)-(4-chlorophenyl)methylene]aniline in Hexane, ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol, and 6000 Poly(ethylene glycol) - **Mark Mangir** EXP285 Determination of the solubility of cinnamic acid in boiling n-hexane to __#|confirm__ results of EXP283 - **Rida Atif** EXP284 Determination of the solubility of benzoic acid in ethylene glycol, diethylene glycol and glyme. -**Valentine Anyiam** EXP283 Determination of the solubility of cinnamic acid boiling in n-hexane - **Rida Atif** EXP282 Recrystallization of cinnamic acid in ethanol/water (50/50 volume).- **Lizzie Clark** EXP281Recrystallization of cinnamic acid in n-hexane - **Rida Atif** EXP280 Determination of solubility of cinnamic acid in methanol via the density method. -**Rida Atif** EXP279 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone and recrystallization in ethyl acetate. -**Matthew McBride** EXP278 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. -**Matthew McBride** EXP277 Determination of solubility of cinnamic acid in ethylene glycol, diethylene glycol and dichloromethane. -**Valentine Anyiam** EXP276 Recrystallization of cinnamic acid using hexane - ** Lacey Condron and Andrew Lang ** EXP275 Determination of solubility of cinnamic acid in methanol via the density method. -**Valentine Anyiam** EXP274 Synthesis of trans-dibenzalacetone from benzaldehyde and acetone. -**Matthew McBride** EXP273 Recrystallization of cinnamic acid in pure ethanol. - **Lizzie Clark** EXP272 To test the solubility of n-[(e)-(4-chlorophenyl)methylene]aniline in ethanol, acetonitrile, benzene, hexane, and THF by the SAMS NMR method.- **Mark Mangir** __EXP271__ Recrystallization of cinnamic acid in ethanol/water. - **Samantha Gaines** EXP270 Determination of the solubility of cinnamic acid in ethylene glycol and propanediol using HNMR method.-**Stephanie Costa** EXP269 Formation of trans-dibenzalacetone from benzaldehyde and acetone. - **Matthew McBride** EXP268 Determination of the solubility of cinnamic acid in ethylene glycol using the density method.-**Stephanie Costa** EXP267 Determination of the solubility of 4-chlorobenzaldehyde in ethanol at room temperature (25C) **Alex Greene** EXP266 Determination of the solubility of cinnamic acid in propylene glycol and glycerol using the density method. **Unnati Hajari** EXP265 Determination of the solubility of cinnamic acid in methanol using the density method. **Unnati Hajari** EXP264 Determination of the solubility of palmitic acid in 2-pentanol using the density method. - **Ashley Sweeney** EXP263 Recrystallization of cinnamic acid in hexane. **-Lacey Condron** EXP262 Recrystallization of cinnamic acid in distilled water.**- Lizzie Clark** EXP261 Determination of the ratio of hemiacetal to 4-chlorobenzaldehyde in ethanol and methanol- **Stephanie Costa** EXP260 Determination of the solubility of 4-chlorobenzaldehyde in ethanol and characterization of possible product using SAMS HNMR method. - **Matthew McBride** EXP259 NMR of 4-chlorobenzaldehyde in ethanol to determine possible presence of other products- **Alex Greene** EXP258 Determination of the solubility of 4-chlorobenzaldehyde in ethanol and methanol.- **Stephanie Costa** EXP257 Determination of the solubility of palmitic acid in methanol using the density method. **- Lizzie Clark** EXP256 Determination of the solubility of palmitic acid in 1-butanol using the density method - **Lacey Condron** EXP255 Determination of the solubility of cinnamic acid in cyclohexanone and 1,2-dichloroethane by the SAMS NMR method. - **Matthew McBride** EXP254 Determination of the solubility of palmitic acid in acetone using the density method - **Lacey Condron** EXP253 Determination of the solubility of palmitic acid in 1-pentanol using the density method. - **Lizzie Clark** EXP252 Determination of the solubility of cinnamic acid in nitromethane using the density method.- **Stephanie Costa** EXP251 Determination of the solubility of trans-cinnamic acid in 1,2 dichloroethane using the density method. - **Alex Greene** EXP250 Determination of the solubility of palmitic acid in 2-butanol using the density method. - **Lizzie Clark** EXP249 Determination of the solubility of palmitic acid in 2-propanol using the density method. - **Lacey Condron** EXP248 Determination of the solubility of palmitic acid in 1-propanol using the density method. - **Lizzie Clark** EXP247 Determination of whether trans-cinnamic acid is miscible in a 5M solution of THF. - **Matthew McBride** EXP246 Determination of the viability of trans-cinnamic acid at concentration 3M in THF - **Alex Greene** EXP245 Determination of the solubility of trans-cinnamic acid in acetonitrile and THF using the density method. - **Matthew McBride** EXP244 Determination of the solubility of trans-cinnamic acid in hexane - **Stephanie Costa** EXP243 Determination of the solubility of cinnamic acid in DMSO and THF - **Stephanie Costa** EXP242 Determination of the solubility of cinnamic acid in cyclohexane, DMSO, and THF - **Stephanie Costa** EXP241 Determination of the solubility of cinnamic acid in 2-butanol - **Lizzie, Lacey, Samantha** EXP240 Determination of the solubility of cinnamic acid in 2-propanol - **Lacey, Lizzie, Samantha** EXP239 Determination of the solubility of cinnamic acid in 2-pentanol - **Samantha, Lacey, Lizzie** EXP238 Determination of the solubility of cinnamic acid in chloroform.- **Stephanie Costa** EXP237 Determination of the solubility of cinnamic acid in Methanol.- **Stephanie Costa** EXP236 Determination of the solubility of trans-cinnamic acid in Benzene, Toluene, and Chloroform using the density method. - **Matthew McBride** EXP235 Ugi synthesis experiment - moved to usefulchem wiki - **Jenna Mancinelli** EXP234 Determination of the solubility of trans-cinnamic acid in acetone using the density method.- **Lacey, Lizzie** EXP233 Determination of the solubility of trans-cinnamic acid in ethyl acetate using the density method.- **Lacey, Lizzie** EXP232 Determination of the solubility of trans-cinnamic acid in propyl acetate using the density method.- **Lizzie, Lacey** EXP231 Determination of the solubility of trans-cinnamic acid in Benzene, Toluene, and Chloroform using the density method. - **Matthew McBride** Exp230 Determination of the solubility of benzoic acid, 4-chlorobenzoic acid and 2-phenylbutyric acid in 2,2,2-trifluoroethanol - **Evan** EXP229 Determination of the solubility of Trans cinnamic acid in Methanol by the density method. - **Matthew McBride** EXP228 Determination of the solubility of Trans cinnamic acid in Benzene, Toluene, Acetonitrile, and Trifluoroethanol by the SAMS NMR method.- **Mark** EXP227 Determination of the solubility of Trans cinnamic acid in Ethanol and Methanol by the SAMS NMR method.- **Mark** EXP226 Determination of the relative concentration of //t//-cinnamic acid in ethanol at different temperatures by density and NMR - **Sozit** EXP225 Determination of the solubility of trans-cinnamic acid in 1-pentanol by density method - **Samantha, Lizzie** EXP224 Determination of the solubility of trans-cinnamic acid in 1-octanol by density method - **Lizzie, Samantha** EXP223 Determination of the solubility of trans-cinnamic acid in 1-butanol by density method - **Samantha, Lacey, Lizzie** EXP222 Determination of the solubility of trans-cinnamic acid in 1-propanol by density method - **Lizzie, Lacy, Samantha** EXP221 Determination of the solubility of trans-cinnamic acid in ethanol by density method - **Lacey, Samantha, Lizzie** EXP220 Determination of the solubility of trans-cinnamic acid in methanol by density method - **Samantha, Lacey, Lizzie** EXP219 Determination of the solubility of Trans cinnamic acid in Ethanol and Methanol by the SAMS NMR method.- **Mark** Exp218 Determination of the solubility of trans-cinnamic aid, salicylic acid, p-dimethylaminobenzaldehyde and vanillin in trifluoroethanol by SAMS HNMR method- **Evan** Exp217 Determination of the solubility of 5 imines in trifluoroethanol by SAMS HNMR method - **Evan** Exp216 Determination of the solubility of 4 imines in 5 solvents. - **Evan** Exp215 Determination of the solubility of benzalaniline in n-hexane, ethyl acetate, isopropanol, dichloromethane, and benzene by SAMS HNMR method **- Evan** Exp214 Determination of the solubility of 4 imines in 90/10 ethanol/water mixture by SAMS HNMR method **- Evan** Exp213 Determination of the solubility of benzalaniline in methanol by SAMS HNMR method - **Evan** Exp212 Determination of solubility of benzalaniline in 5 solvents by SAMS HNMR method - **Evan** Exp211 Determination of solubility of cinnamic acid in (several solvents) by density method - **Mary** Exp210 Determination of solubility of 2-phenylbutyric acid in //n//-hexane by density method - **Ha Pham** Exp209 Determination of solubility of cinnamic acid in ethanol by density method- **Mary** Exp208 Determination of solubility of cinamic acid in methanol and ethanol by density method - **Evan and Ha** Exp207 Determination of solubility of sample 1A from UCExp262 in toluene, acetonitrile, THF, and chloroform - **Evan** Exp206 Determination of solubility of sample 1A from UCExp262 - **Evan** Exp205 Determination of solubility of benzalaniline in 5 solvents - **Evan** Exp204 Determination of solubility of 2-phenylbutyric acid in //n//-hexane by density method. **- Evan** Exp203 Determination of solubility of 2-phenylbutyric acid in //n//-hexane, 2-propanol, and methanol by NMR. - **Sozit** Exp202 Determination of solubility of //trans//-cinnamic acid in methanol using the density method. - **John** Exp201 Determination of solubility of 2-phenylbutyric acid in methanol by density method. - **Evan** Exp200 Determination of solubility of //trans//-cinnamic acid in methanol using the density method. - **John** Exp199 Determination of solubility of Benzoic acid in chloroform, methanol and Hexane by density method. - **Jianbo** Exp198 Determination of solubility of salicylic acid in chloroform, water and acetonitrile by density method. - **Evan** Exp197 Determination of solubility of //trans-//cinnamic acid in methanol by density method. - **Evan** Exp196 Determination of the concentration of Exp193-Sample3 by NMR and density methods. - **Sozit** Exp195 Determination of the solubility of boc-alanine and boc-phenyl alanine in hexane, acetonitrile, methanol, t-butanol and benzene by the [|SAMS method] - **Khalid** Exp194 Determination of the solubility of boc-alanine and boc-phenyl alanine in hexane, acetonitrile, methanol, t-butanol and benzene by the [|SAMS method] - **Khalid** Exp193 Observation of solubility of 2-phenylbutyric acid in hexanes in different temperature(up to 45C) - **Jianbo** Exp192 Determination of solubility of 2-phenylbutyric acid in three pure solvent ( benzene, methanol and hexene) at variable time in volumetric flasks-**Jianbo** Exp191 Observation of solubility of benzaldehyde in n-hexane through melting point - **Sozit** Exp190 Observation of solubility of t-butanol in n-hexane through melting point - **Sozit** Exp189 Determination of solubility of piperonal in n-hexane at different temperatures using NMR - **Sozit** Exp188 Observation of solubility of piperonal in hexanes through melting point - **Jianbo** Exp187 Observation of solubility of piperonal in n-hexane in different temperature(up to 40C)- **Jianbo** Exp186 Determination of solubility of piperonal in n-hexane using four sizes of volumetric flasks - **Jianbo** Exp185 Observation of solubility of piperonal in n-hexane through melting point - **Sozit** Exp184 Observation of solubility of cyclohexanecarboxylic acid in hexanes through melting point - **Sozit** Exp183 Determination of solubility of cyclohexanecarboxylic acid in hexane at 25C and 0C - **Jianbo** Exp182 statistically analyze the differences between methanol densities measured under different flask volumes- **Wei** Exp181 Determination of error in different volumetric flasks using methanol and the density method - **Jianbo** Exp180 Determination of error in different volumetric flasks using methanol and the density method - **Sozit** Exp179 Determination of density of pure methanol in different flasks at room temperature - **Jianbo** Exp178 Determination of solubility of different concentrations of cinnamic acid in methanol at room temperature - **Sozit** Exp177 Determination of solubility of cinnamic acid in methanol at variable time in volumetric flasks-**Jianbo** Exp176 Determination of solubility of cinnamic acid in methanol using four sizes of volumetric flasks - **Sozit** Exp175 Determination of solubility of cinnamic acid in several solvents - **Imran** Exp174 Determination of solubility of different solutes heated at variable times - **Imran** Exp173 Verifying the density method of cinnamic acid in methanol using QCM - **Imran** Exp172 Determination of the solubility of several solutes by density - **Imran** Exp171 Determination of solubility of cinnamic acid in methanol - - **Jessica** Exp170 Verifying the density method of cinnamic acid in methanol - **Jessica** Exp169 Verifying the density method of cinnamic acid in methanol - **Imran** Exp168 Verifying the density method of cinnamic acid in methanol - **Jessica** Exp167 Determination of the solubility of Ugi 176C in EtOAc and phenanthrene-9-carboxaldehyde in THF - **Khalid** Exp166 Effect of the three co-solutes on the solubility of the Ugi product UC176C in ethyl acetate - **Khalid** Exp165 Determination the solubility of phenanthrene-9-carboxaldehyde, phenylacetic acid and the 176C(UC) in ethyl acetate by SAMS - **Khalid** Exp164 Determination of the solubility of 2,6 dicholobenzaldephyde in DMSO and benzene using SAMS - **Alisha** EXP163 Determination of the solubility of benzoic acid in absolute ethanol using density measurements- **Harina** Exp162 Determination of the solubility of benzoic acid in methanol using density measurements - **Alisha** Exp161 Determination of the solubility of Ugi 234 in ethanol by gravimetric analysis - **David** Exp160 Determination of solubility of benzoic acid in ethanol by gravimetric analysis - **David & Chau** Exp159 Estimation of the concentration of Ugi product (UC176C) left dissolved in a supernatant of its reaction - **Khalid** Exp158 Effect of butylisocyanide concentration on the solubility of the Ugi product UC176C in benzene - **Khalid** **&** **Hai** Exp157 Effect of phenylacetic acid concentration on the solubility of the Ugi product UC176C in benzene - **Khalid** Exp156 Effect of imminium concentration on the solubility of the Ugi product UC176C in benzene - **Khalid** Exp155 Determination of solubility of benzoic acid, phenylacetic acid and the Ugi product UC176C in 1-octanol - **Khalid & Hai** Exp154 Effect of phenylacetic acid on the solubility of the Ugi product UCExp176C at lower concentration (0.01M - 0.5) in benzene - **Hai & Khalid** Exp153 Effect of imminium concentration on the solubility of the Ugi product UC176C in methanol - **Hai & Khalid** Exp152 Effect of imminium concentration on the solubility of the Ugi product UC176C in benzene - **Hai & Khalid** Exp151 To measure the solubility of Ugi product UCExp176C in methanol with a) ~0.05 imine b) imine + phenylacetic acid. **Hai & Khalid** Exp150 To measure the solubility of Ugi product UCExp176C in solution of benzene and a) phenanthrene-9-carboxaldheyde, furufylamine and phenylacetic acid as cosolutes **Hai & Khalid** Exp149 To measure the solubility of Ugi product UCExp176C in 0.1M, 0.2M, 0.3M, 0.5M imine solution in benzene **Hai & Khalid** Exp148 Determination of solubility of UC176C in a 0.1M imine solution in benzene b) 0.1M n-butylisocyanide solution in benzene - **Hai & Khalid** Exp147 Effect of phenylacetic acid and fufurylamine (equimolar solutions) in benzene on the solubility of the Ugi product Exp146 Effect of phenylacetic acid concentration on the solubility of the Ugi product UC176C in benzene - **Khalid** Exp145 Determination of solubility of Ugi product UC148B in benzene, THF, acetonitrile, methanol and ethanol - **Khalid & Hai** Exp144 Effect of starting materials on the solubility of Ugi product UC176C in benzene - **Khalid & Hai** Exp143 Determination of solubility of boc-glycine in 2-propanol, benzene - **Khalid & Hai** Exp142 Determination of solubility of salicylic acid in chloroform - **Hai & Ciana** Exp141 Determination of solubility of salicylic acid in chloroform - **Ciana** Exp140 Determination of solubility of salicylic acid in toluene - **Ciana** Exp139 Determination of solubility of salicylic acid in toluene - Ciana Exp138 Determination of the solubilities of four solutes in different solvents by NMR - **Jenna Mancinelli** Exp137 Determination of the solubility of 4-acetamidobenzoic acid and nicotinic acid in five solvents - **Khalid** Exp136 Determination of the solubilities of seven solutes in different solvents by NMR - **Jenna Mancinelli** Exp135 Continuation of solubility-temperature study of Boc-Glycine in THF - **Jenna Mancinelli** Exp134 Determination of solubility for Cbz-L-Proline in methanol - **Khalid** Exp133 Determination of solubility-temperature curve for Boc-Glycine in THF - **Jenna Mancinelli** Exp132 Determination of solubility of 3,4-(methylenedioxy)phenylacetic acid in methanol - **Khalid** Exp131 Determination of solubility of 3,4-(methylenedioxy)phenylacetic acid in THF - **Khalid** Exp130 Solubility-Temperature study of 4-nitrobenzaldehyde, Continued - **Marshall Moritz** Exp129 Determination of solubility of 3,4-(methylenedioxy)phenylacetic acid in many solvents-**Dan Rein** Exp128 Generation of solubility-temperature curve for 4-nitrobenzaldehyde in four solvent mixture - **Jenna Mancinelli** Exp127 Compound 237-1B (176C) solubility in different sovents at 23 degrees C.**- Anthony Shorrock** Exp126 **DOSOL** Temperature study of benzoic acid in methanol-**Dan Rein** Exp125 **DOSOL** Determination of solubility of Ugi product UCExp235-2A in different solvents by NMR- **Khalid, Jenna** Exp124 **DOSOL** Temperature study of 3,4 methylenedioxyphenylacetic acid in acetonitrile- **Matthew Federici** Exp123 Determination of solubility of phenylacetic acid in 4 different solvents by NMR and recrystallization methods - **Marshall Moritz** Exp122 Solubility-Temperature study of 4-nitrobenzaldehyde, Continued - **Marshall Moritz** __Exp121__ Temperature study of 4-fluorobenzoic acid in ethanol-**Dan Rein** Exp120 Temperature study of 4-fluorobenzoic acid in ethanol- **Dan Rein** Exp119 Temperature study of 3,4 methylenedioxyphenylacetic acid in methanol- **Matthew Federici** Exp118 **DOSOL** Temperature study of benzoic acid in methanol - **Anthony Shorrock** Exp117 **DOSOL** Temperature study of BOC-Glycine and THF at specific concentrations-**Daniel Rein** Exp116 Temperature study of BOC-Glycine and THF-**Daniel Rein** Exp115 Verification of the SAMS using varying concentrations of benzoic acid in DMF - **David** Exp114 Constucting a solubility curve for 4-nitrobenzaldehyde in a 4-solvent system - **Marshall Moritz** Exp113 Determination of solubility of Ugi product UCExp216-3A in different solvents by NMR- **Jenna** Exp112 Generating a solubility-temperature curve of pyrene in acetonitrile - **Jenna** Exp111 Generating a solubility-temperature curve for 4-nitrobenzaldehyde in acetonitrile and chloroform by recrystallization - **Marshall Moritz** Exp110 Generating a solubility-temperature curve for 4-nitrobenzaldehyde in methanol by recrystallization - **Marshall Moritz** Exp109 Construction of a solubility curve for pyrene in acetonitrile by cooling crystallization method - **Khalid, Dr. Bradley, Cedric** Exp108 Determination of the solubility of pyrene in acetonitrile - **Marshall Moritz** Exp107 Determination of the solubility of p-toluenesulfonic acid in toluene and acetonitrile - **Marshall Moritz** Exp106 Determination of the solubility of p-Fluorobenzoic acid in six different solvents - **Marshall Moritz** Exp105 Determination of the solubility of 2-chloro-5-nitrobenzaldehyde in six different solvents - **Marshall Moritz** Exp104 Determination of the solubility of furoic acid in five different solvents - **Marshall Moritz** Exp103 Verification of the SAMS method using varying concentrations of 1-pyrenebutyric acid in different solvents - **Khalid** Exp102 Verification of the SAMS method using varying concentrations of 2-phenylbutyric acid in DMSO - **David** Exp101 Determination of 0.6 __M__ solution of 4-pyrenebutanoic acid in 0.4347:1.000 solution of THF:ethanol - **David** Exp100 Determination of the solubility of nicotinic acid in 5 different solvents - **Marshall Moritz** Exp099 Determination of the solubility of 4-pyrenebutanoic acid in DMF and DMSO - **David** Exp098 **DOSOL** Determination of the solubility of eight solutes in methanol, acetonitrile, and DMSO - **Matthew Federici** Exp097 Determination of the solubility of Ugi product 216-4A in 5 different solvents - **Matthew Federici** Exp096 Determination of the solubility of Ugi product 216-7A in 6 different solvents - **David** Exp095 Determination of the solubility of chloroacetic acid in 5 different solvent - **Marshall Moritz** Exp094 Verification of the SAMS method using a 2.81 __M__ solution of 2-phenylbutyric acid in THF - **David** Exp093 Determination of the solubility of Ugi product 216-4A in methanol, ethanol, and acetonitrile- **Cedric** Exp092 Determination of the solubility of 4-methoxyphenylacetic acid in THF (verification) - **David** Exp091 Determination of the solubility of 4-pyrenebutanoic acid in THF (verification) - **David** Exp090 Determination of the solubility of 2,3-Dihydroxybenzoic acid in 6 different solvents- **Shuba** Exp089 Determination of the solubility of 4-methoxyphenylacetic acid in 5 different solvents - **Marshall Moritz** Exp088 Determination of the solubility of 4-hydroxybenzaldehyde in THF - **Marshall Moritz** Exp087 Determination of solubility of 2,4,6-Trihydroxybenzoic acid in 6 different solvents- **Shuba** Exp086 Determination of the solubility of phenylacetic acid in acetonitrile and toluene- **Cedric** Exp085 Determination of the solubility of six solutes in THF - **Matthew Federici** Exp084 Determination of the solubility of 4-pyrenebutanoic acid in THF (verification) **Khalid** Exp083 Determination of the solubility of 2-phenylbutyric acid in toluene, THF, and DMSO by NMR spectroscopy- **Cedric** Exp082 Determination of the solubility of six solutes in THF - **Matthew Federici** Exp081 Determination of the solubility of dipheylacetic acid in six solvents - **Khalid, Shuba** Exp080 Determination of the solubility of 2-phenylbutyric acid in DMSO, THF, and toluene- **Cedric** Exp079 Determination of the solubility of 2-phenylbutyric acid in ethanol and acetonitrile by NMR spectroscopy- **Cedric** Exp078 Determination of the solubility of one Ugi product in six solvents - **Matthew Federici** Exp077 Determination of the solubility of Diphenylacetic acid in methanol - **Matthew Federici** Exp076 Determination of the solubility of two Ugi products in six solvents - **Shuba**, **Khalid** Exp075 Determination of the solubility of 4-chlorophenylacetic acid in seven solvents - **Shuba**, **Khalid** Exp074 Exp073 Determination of the solubility of 4-chlorophenylacetic acid in methanol and THF using 2 methodologies by NMR- **Cedric** Exp072 Determination of the solubility of DL-mandelic acid, trans-cinnamic acid, 4-phenylbutyric acid, L-ascorbic acid, acetylsalicylic acid and 4,4-azoxydibenzoic acid in various solvents using ** 1 **H NMR - **David**
 * UC176C** - **Khalid**
 * (DOSOL)** Determination of the solubility of 4-pyrenebutanoic acid in THF and a 3:1 mix of THF and methanol - **Khalid**

Exp071 Determination of the solubility of the Ugi product UC215C, vertatraldehyde, piperonal and Boc-glycine in different solvents - **Khalid** Exp070 **(DOSOL)** Determination of the solubility of Octadecylamine and 5 solvents - **HaeJi** Exp069 Determination of the solubility of Octadecylamine and 5 solvents - **HaeJi** Exp068 **(DOSOL)** Determination of the solubility of TOSMIC and octadecylamine in acetonitrile - **Khalid** Exp067 Verifying the concentrations of 0.25M 4-pyrenebutanoic acid solution and 1.25M crotonic acid solution in DMSO by HNMR- **Khalid, Cedric** EXP066 JennyHale-16: Measuring the solubility of 8-bromo-octanoic acid in ethanol - **Jenny** Exp065 Determination of the solubility of eleven Ugi products in methanol by HNMR - **Khalid** Exp064 Determination of the solubility of crotonic acid in acetonitrile, chloroform, ether, DMSO, and n-hexane by NMR -**Cedric** EXP063 JennyHale-15: Measuring the solubility of the liquid aldehydes 3,5-dimethylbenzaldehyde and 4-ethylbenzaldehyde in ethanol, methanol and THF by miscibility and density calculations. - **Jenny** Exp062 Determination of the solubility of crotonic acid in methanol, THF, benzene, ethanol, and toluene by NMR -**Cedric** Exp061 Determination of the solubility of the 4-pyrenebutanoic acid sixteen solvents - **Khalid** Exp060 Determination of the solubility of the phenanthrene-9-carboxaldehyde in sixteen solvents - **Khalid** EXP059 JennyHale-14 : Measuring the solubility of liquid aldehyde 3,4-dimethylbenzaldehyde in ethanol, methanol and THF - **Jenny** EXP058 JennyHale-13: Measuring the solubilities of benzoic acid and undecanoic acid in ethanol, methanol and THF. Re-measuring the solubility of 4-hydroxybenzaldehyde in THF. - **Jenny** EXP057 JennyHale-12: Measuring the solubilities of 10-chloro-9-anthraldehyde; 4-hydroxybenzaldehyde and 4-hydroxy-3-methylbenzaldehyde in ethanol, methanol and THF - **Jenny** Exp056 Determination of the solubility of the Ugi product [|UC206B] in seventeen solvents - **Khalid** Exp055 Determination of the solubility of Vanillin in Ethanol - **DU students** Exp054 Determination of the solubility of Succinic Acid in Ethanol - **DU students** Exp053 Determination of the solubility of Urea in Methanol - **DU students** Exp052 Determination of the solubility of Salicylic Acid in Methanol - **DU students** Exp051 Determination of the solubility of Phenanthrene-9-carboxaldehyde & 1-pyrenebutyric acid in DMSO by NMR - **Khalid** Exp050 Determination of the solubility of Vanillin in Ethanol - **DU students** Exp049 Determination of the solubility of Citric Acid Monohydrate in Water - **DU students** Exp048 Determination of the solubility of Cinnamic Acid in Methanol - **DU students** Exp047 Determination of the solubility of Phthalic Acid in Methanol - **DU students** Exp046 Determination of the solubility of Riboflavin in Methanol - **DU students** Exp045 Determination of the solubility of Succinic Acid in Isopropanol - **DU students** Exp044 Determination of the solubility of Succinic Acid in Ethanol - **DU students** Exp043 Determination of the solubility of Benzoic Acid in Methanol - **DU students** Exp042 Determination of the solubility of Succinic Acid in Ethanol - **DU students** Exp041 Determination of the solubility of 3,4-Dimethoxybenzaldehyde in Acetone - **DU students** Exp040 Determination of the solubility of Maleic Acid in Methanol - **DU students** Exp039 Determination of the solubility of Maleic Acid in Ethanol - **DU students** Exp038 Determination of the solubility of Tartaric Acid in Acetone - **DU students** Exp037 Determination of the solubility of Benzoic Acid in Acetone - **DU students** Exp036 Determination of the solubility of Salicylic Acid in Ethanol **- DU students** Exp035 Determination of the solubility of Acetanilide in Acetone - **DU students** EXP034 Determination of solubility of salicylic acid, acetylsalicylic acid, and o-anisic acid in protonated chloroform. - **David** Exp033 Determination of solubility of veratraldehyde , 4-dimethylaminobenzaldehyde , 4-chlorobenzaldehyde, 2,6-dichlorobenzaldehyde, 2-chloro-3-nitro-benzaldehyde and 4-nitrobenzaldehyde in methanol. - **Cedric & Khalid** EXP032 (JennyHale-11) Repeat of JennyHale-3: Measuring the solubilities of benzotriazole-5-carboxylic acid; 8-bromooctanoic acid; 4-dimethylaminocinnamaldehyde and 2-(4-hydroxyphenyl)azobenzoic acid in ethanol and methanol. - **Jenny** EXP031 Confirming the solubility of Benzoic acid in Chloroform using ** 1 **H NMR - **David** EXP030 Determination of solubility of Phenanthrene-9-carboxaldehyde, 1-pyrenebutyric acid and piperonal in different solvents by NMR- **Khalid** Exp029 Determining the solubility of Octylamine, Cyclohexylamine, Benzylamine, Aniline, and //o//-Chloroaniline in Methanol using different combination analysis -**Cedric** EXP028 Proton NMR Integral Ratio Comparision using 4-Chlorobenzaldehyde in Chloroform-//d// - **David**

Exp027 Determination of solubility of Phenanthrene-9-carboxaldehyde in methanol by NMR- **Khalid** Exp026 Determining the solubility of Furfurylamine and 5-Methyl-2-Furanmethanamine in Methanol using different combination analysis -**Cedric**

EXP025 (JennyHale-10) Repeat of JennyHale-2: Measuring the solubilities of citric acid, 2-oxoglutaric acid, sinapic acid and p-Toluic acid in ethanol, methanol and THF - **Jenny**

Exp024 Determination of solubility of Phenanthrene-9-carboxaldehyde and 1-Pyrenebutyric acid in methanol by UV-Vis - **Khalid** Exp023 Determination of solubility of 2-naphthaldehyde, 4-hydroxybenzaldehyde, 4-nitrobenzaldehyde, //o//-vanillin and piperonal in methanol by UV-Vis -**Khalid** Exp022 Determination of solubility of 19 liquid carboxylic acids and 2 aldehyes in methanol -**Khalid** Exp021 Determination of solubility of fourteen liquid aldehydes in methanol -**Khalid** Exp020 Determination of solubility of 2-furaldehyde in methanol -**Khalid** Exp019 Determination of solubility of vanillin in methanol by UV-Vis -**Khalid** Exp018 Determination of extinction coefficient of vanillin in methanol (UV) - **Khalid** EXP017 Solubility determination procedure for 4-chlorobenzaldehyde in non-deuterated chloroform by proton NMR using sonicator- **David** EXP016 Solubility determination procedure for 4-chlorobenzaldehyde in non-deuterated chloroform by proton NMR - **David** EXP015 (JennyHale-9) Measuring the solubility of 4-hydroxyphenylpyruvic acid, 11-mercapto-undecanoic acid and 4-nitrophenylacetic acid in ethanol and methanol - **Jenny** EXP014 (JennyHale-8) Measuring the solubility of 1-adamantylamine and 6-aminocaproic acid in ethanol and methanol - **Jenny** EXP013 (JennyHale-7) Study of Temperature effect on solubility of vanillin in methanol and ethanol 3 - **Jenny** EXP012 Determining the extinction coefficient of 4-chloroenzaldehyde via UV/VIS.**- Tim** EXP011 (JennyHale-6) Study of Prolonged Vortexing time solubility of vanillin in methanol and ethanol - **Jenny** EXP010 (JennyHale-5) Study of Temperature effect on solubility of vanillin in methanol and ethanol 2 - **Jenny** EXP009 Solubility of benzoic acid in toluene- **Cedric** EXP008 (JennyHale4) Study of Temperature effect on solubility of vanillin in methanol and ethanol - **Jenny** EXP007 Solubility of benzoic acid and 4-chlorobenzoic acid in varying solvents.- **Tim** EXP006 Solubility of 4-chlorobenzaldehyde in chloroform and methanol by UV spectroscpy - **Khalid** EXP005 Solubility of benzoic acid in methanol - **Cedric** EXP004 Speedvac on phenanthrene-9-carboxaldehyde, 4-chlorophenylacetic acid, and vanillin- **Tim** EXP003 (JennyHale 3) - **Jenny** EXP002 (JennyHale-2) - **Jenny** EXP001 (JennyHale-1) - **Jenny**

=List of Solubility Experiments on UsefulChem= UC-EXP212 (Tim Bohinski) speedvac on 4-nitrobenzaldehyde UC-EXP211 (Khalid Mirza) UV on 4-chlorobenzaldehyde UC-EXP210 (Khalid Mirza) UC-EXP209 (Khalid Mirza and Tim Bohinski) UC-EXP208 (Khalid Mirza and Tim Bohinski) UC-EXP207 (Jean-Claude Bradley and Cameron Neylon) UC-EXP205 (Khalid Mirza and Tim Bohinski)

= Researcher = Alex Greene = Objective = To determine if trans-cinnamic acid can be made into a 3.0 M concentration in the solvent THF using a 5ml volumetric flask = Procedure = Cinnamic acid was measured to on a balance to have a concentration of 3M in a 5ml volumetric flask. The Cinnamic acid was added to a volumetric flask. Then THF was added to the flask up to the 5ml mark on the volumetric flask. = Results = The Cinnamic acid failed to completely dissolve in the THF at room temperature with mixing by inverting and sonication. Undissolved cinnamic acid remained at the bottom of the volumetric flask. = Discussion = = Conclusion = The Cinnamic acid failed to completely dissolve in the solution of THF. The result is a contradiction of EXP 245, which had a cinnamic acid concentration around 3M = Log =

2012-01-11
11:17- A 5ml volumetric flask was weight at 23.7969g 11:20- 2.2260g of trans-cinnamic acid was weighted and transferred to volumetric flask 11:28- THF was added to volumetric flask up to 5ml mark 11:34- Inverted flask repeatedly for 8 seconds to mix solution 11:35- Sonicated flask for 5 seconds 11:38- Took picture #1